Preparation of 1-deuterioaldehydes via tub use of diisobutylaluminum deuteride (DIBAL-D)
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چکیده
منابع مشابه
Preparation and Purification of Hydrogen Deuteride
In an investigation of t he physical properties of hydr<;>gen isotopes it was n.ecessar.\:' t o prepare 10 liters of high-purity. hydro~en d~u.tende. TI1JS was don e ~y r eactmg IJ t hlUm aluminum hydride wit h deutenum oXIde, gly.;n~ hydro~en deutende, ]I) .t wo batch~s, ?f 98.1and 97.0-percent purity, respect ive!.\:' . .Ihls mater!ai was t hen frac t IOnated at JtqUJd hydrogen t emperature i...
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ژورنال
عنوان ژورنال: Tetrahedron
سال: 1984
ISSN: 0040-4020
DOI: 10.1016/s0040-4020(01)91486-3